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In extracts’ analysis for residual solvents, the most efficient method is the Headspace Gas Chromatography/Mass Spectroscopy (GC/MS) technique. The sealed vial containing the sample is heated, exciting the molecules to a gas phase. It is performed by dissolving the sample in a high-molecular-weight compound such as dimethylformamide before placing it in a headspace vial. It is also important that the compound to be extracted should have greater solubility in the solvent that has been added, and that this should not dissolve any unwanted substances in the original mixture. The choice of solvent to be used will depend on the chemical and physical properties of all the substances in the mixture. The drug 2C-B was created by chemist Dr Alexander Shulgin, credited with the discovery of other mind-altering substances including MDMA. Several supercritical fluids have been either banned or are under strict regulations because of their hazardous effects on the health and environment, including Nitrous oxide, Ethylene dioxide, Ethane, and Benzene. Of all types, the standard FDA-approved solvent for extraction is carbon dioxide, as a result of its eco-safety and high purity. The R134a “tetrafluoroethane” extraction is a novel technique similar to Carbon dioxide extraction, discovered by COMERG. Though pioneered by R134a, this method is efficient with carbon dioxide extraction to eliminate the need for further procedures; R134a extracts terpenes and live resins in10-15 minutes, while ethanol separates cannabinoids in about 30-60 minutes.
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